Cal state La NMR

Cal Sate La NMR Facility

 

Instruction to NMR

 

 

Facility manager and Staffs

 

NMR Facility Tour

 

Cal State La NMR Users Guide

 

Maintenance Schedule

 

Experiment Reservations

 

NMR cost

 

Training Procedure

 

Operational Status


Publications & Presentation

 

Current NMR Research at Cal state La

 

Other NMR WWW sites

 

Cal state La University

 

Department of Chemistry

 

 

 

 

 

 

 

 

 

Facility manager and Staffs

 

Dr. Yong Ba  

(NMR Facility Manager & Chemistry Professor)

Phone: (323) 343-2360            Email : yba@exchange.calstatela.edu

 

Dr. Ali Jabalameli

(NMR Facility Assistant Manager &  NMR specialist)

Phone: (323) 343-2320            Email: ajabala@calstatela.edu

 

Alvaro R. Beas

(NMR Computer Administrative & Communication Instructional Technician)

Phone: (323) 343-2320         Email: abeas3@exchange.calstatela.edu

 

Keith Clark

(NMR maintenance staff & Technician III)

Phone: (323) 343-2318         Email: kclarke@exchange.calstatela.edu

 

Floyd Nesbitt

(NMR maintenance staff &Technician III)

Phone: (323) 343-2367          Email: fnesbit@exchange.calstatela.edu

 

 

 

NMR Facility Tour

 

 

·        NMR Facility Laboratory

·        Bruker 300 NMR Spectrometer

·        Bruker DRX 400 NMR Spectrometer

·         ? 600 NMR Spectrometer

·        Staff Offices

 

 

 

 

 

 

 

 

 

 

 

 

Cal State La NMR Facility Users Guide

 


Preparation & Spectrometer Operation , Acquisition , Processing , Printing , and Miscellaneous

Preparation and Spectrometer Operation

Liquid-State

1.   Introduction

2.   Preparing of NMR sample

3.   Setting up the Spectrometers

4.   Tuning the Probes

5.   locking and shimming

6.   Calibrating a 90° pulse

7.   Relaxation Times

8.   Variable Temperature Operation

Solid-State

1.   Introduction

2.   Preparing of NMR sample

3.   Setting up the Spectrometers

4.   Tuning the Probes

Acquisition

1D NMR Experiments

1.   The basic parameters for a 1D experiment

2.   1H one-pulse experiment

3.   13C one-pulse experiment

4.   Homonuclear decoupling

5.   Signal Suppression

6.   1D NOE experiment

7.   DEPT

8.   C13DEPT

9.   T1 inversion-recovery experiment

10. 1H with 19F decoupling

11. 19F with 1H decoupling

12. Homonuclear decoupling on X nuclei

13. 13C with 1H and 2H decoupling

14. Other double resonance experiments

2D NMR Experiments

1.   COSY

3.   phase-sensitive COSY

4.   MQ COSY

5.   TOCSY

6.   NOESY

7.   HOM2DJ

8.   HET2DJ

9.   HETCOR or HMQC?

10. HETCOR

11. phase sensitive HETCOR

12. Long-Range HETCOR

13. HMQC

14. HMBC

15. INADEQUATE

Processing

1.   Processing 1D spectra

2.   Processing 2D spectra

3.   Linear Prediction

4.   Baseline Correction 5.  Peak Picking

6.   Integration

 

 

 

 

 

 

 

 

Printing

1.   How do I plot my spectrum ?

2.   How do I change the font size on my parameters ?

 

3.   How do I print pick print and integration ?

4.   How do I print a stacked spectrum ?

5.   How do I plot a 2D homonuclear correlation (COSY, NOESY, TOCSY, etc.) type spectrum?

6.   How do I plot a 2D heteronuclear correlation (HETCOR, HMQC, HMBC, etc.) type spectrum?

Miscellaneous

  1. How to Change your Password
  2. NMR Solvents

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Maintenance Schedule

 

·        Bruker 300 NMR Spectrometer

·        Bruker DRX 400 NMR Spectrometer

·         ? 600 NMR Spectrometer